Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method
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Abstract
In this study,the nanoparticles of zinc oxide were readily prepared through Hydrothermal process by using zinc nitrate hexahydrate, and Sodium hydroxide as aprecursors. The surface topology, and crystalline structure of prepared ZnO nanoparticles were studied. X-ray diffraction (XRD) revealed that the prepared ZnO nano particles is highly crystalline, having (wurtzite) crystal structure. The optical analysis by UV–vis showed that these ZnO nano particles have considerable blue shift in the optical band gap energy (Eg = 4.9eV), and this may be to the quantum confinement effect of nano particles. The FT-IR results shows the existence of OH, COO, H2O groups the characteristic vibrational modes of Zn–O were identified. and AFM analysis showed that the diameters of the ZnO particles is in ananometer range of (70-74)nm
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References
[1] Almoqayyad, S .I. (2012). Study of Synthesis and Growth of ZnO Nanoparticles. M,Sc.thesis, Al-Azhar University of Gaza.
[2] Idris, W.A. (2015). Characterization of Nanostructure ZnO synthesized through hydrothermal method, M.Sc. thesis, University of Tun Hussein Onn Malaysia.
[3] Chowska, K .Z. (2014). Methods of ZnO nanoparticles synth-esis. Journal of Biotechnology, Computational Biology and Bio nanotechnology, 95(2):150-159.
[4] Amin, G. (2012). ZnO and CuO Nanostructures; low tempera-ture growth Characterization, Their Optoelectronic and Sensing Applications. M,Sc. thesis, Linköping University.
[5] Kolekar, T.V.et al. (2013). Synthesis and characterization of ZnO nanoparticles for efficient gas sensors. Archives of applied Science research, 5 (6):20-28.
[6] Teklemichael, S.T. (2012). Defects in zinc oxide nanocrystal. Ph. D. thesis, Washington state University.
[7]-Kumar, H. (2013). Structural and optical characterization of ZnO Nanoparticles synthesized by micro emulsion route. International letters of chemistry; physics and astronomy, 14: 26-36
[8] Reddy, A.R. (2015). Hydrothermal synthesis and characterization of ZnO nano Crystals. International journal of minning and metallurgy , 3(2): 52-56.
[9] Vinosel, V. M. et al. (2017). Facile synthesis of CuO nano particles by hydrothermal method and their application on their antibacterial activity. International research Journal of enginering and Technology, 4(8): 106-109
[10] Poole, C.p. (2003). Introduction to nanotechnology. John Wiley and sons, Inc.
[11] Kulkarni, S.S. (2015). Optical and Structural properties of zinc oxide Nanoparticles. international journal of advanced research in physical science , 2(1):14-18.
[12] Alwan, M.A. et al. (2015). Synthesis of zinc oxide Nanoparticles Sol Gel route and their charecterization. Nanoscience and technology, 5(1): 1-6
[13] Munoz, M.M. et al. (2017). Shape-control of zinc oxide Nanoparticles; enhancing photocatalytic activity under UV irradiation. International Congressof Engineering physics, IOP pulishing. series 792/ 012068.
[14] Kannaki, K. et al. (2012). Hydrothermal synthesis of CuO Nano structure and their Charecterizations. International journal of Scientific and engineering research, 3(9): 1- 4.